tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate

Base Information

Chemical Name:tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate
CAS No.:1319069-11-8
Molecular Formula:C₁₆H₂₂N₂O₅
Molecular Weight:322.361
Hs Code.:

Synonyms:tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate

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Technology Process of tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate

There total 2 articles about tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 1319069-10-7
(2-Oxo-ethoxy)-phenyl-acetic acid methyl ester

: 1319069-11-8
tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate

Guidance literature:: In toluene; at 65 ℃;

Reference yield:

: 114209-14-2
(1-allyloxy-1-methoxymethyl-but-3-enyl)-benzene

: 1319069-11-8
tert-butyl 2-(2-(2-methoxy-2-oxo-1-phenylethoxy)ethylidene)hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ozone / dichloromethane / -75 °C

1.2: 12 h / 20 °C / Inert atmosphere

2.1: toluene / 65 °C

With ozone; In dichloromethane; toluene;