diallylphenylphosphino-borane

Base Information

Chemical Name:diallylphenylphosphino-borane
CAS No.:259752-60-8
Molecular Formula:C₁₂H₁₈BP
Molecular Weight:204.06
Hs Code.:

Synonyms:diallylphenylphosphino-borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diallylphenylphosphino-borane

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Technology Process of diallylphenylphosphino-borane

There total 1 articles about diallylphenylphosphino-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 13292-87-0
dimethyl sulfide borane

: 644-97-3
Dichlorophenylphosphine

: 1730-25-2
allylmagnesium bromide

: 259752-60-8
diallylphenylphosphino-borane

Guidance literature:: In diethyl ether; BH3*(CH3)2S in diethyl ether was added dropwise with stirring to a soln.of PhPCl2 in diethyl ether at 0°C, stirred for 45 min, added dro pwise to (allyl)MgBr in diethyl ether, warmed to room temp., stirred for1.5 h (Ar); H2O was added, extd. with diethyl ether, washed with water, aq. satd. NaCl, dried (MgSO4), evapd. under vac., flash column chromy. (petroleum ether-toluene); as oil;
DOI:10.1039/b306940k

Reference yield: 58.0%

: 259752-60-8
diallylphenylphosphino-borane

: C₁₂H₂₀BP

Guidance literature:: diallylphenylphosphino-borane; With n-butyllithium; zirconocene dichloride; In tetrahydrofuran; at 20 ℃; for 12h;

With hydrogenchloride; In water; at 20 ℃; for 0.25h;
DOI:10.1016/S0040-4020(99)00780-2

Reference yield:

: 259752-60-8
diallylphenylphosphino-borane

: 259752-65-3,260047-55-0,260047-56-1
C₁₂H₁₈BBr₂P

Guidance literature:: diallylphenylphosphino-borane; With n-butyllithium; zirconocene dichloride; In tetrahydrofuran; at 20 ℃; for 12h;

With bromine; In tetrahydrofuran; tetrachloromethane; at -78 ℃;
DOI:10.1016/S0040-4020(99)00780-2