2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

Base Information

Chemical Name:2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride
CAS No.:1366348-97-1
Molecular Formula:C₁₉H₂₀ClN₃S*ClH
Molecular Weight:394.368
Hs Code.:

Synonyms:2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

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Chemical Property of 2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

Chemical Property:

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Technology Process of 2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

There total 3 articles about 2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 37859-43-1
2-chloromethylbenzothiazole

: 41885-98-7
1-(4-chlorophenyl)homopiperazine

: 1366348-97-1
2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

Guidance literature:: 2-chloromethylbenzothiazole; 1-(4-chlorophenyl)homopiperazine; With potassium carbonate; potassium iodide; In 1,2-dimethoxyethane; for 16h; Reflux; Inert atmosphere;

With hydrogenchloride;
DOI:10.1016/j.bmc.2012.01.022

Reference yield:

: 505-66-8
1,4-Diazacycloheptane

: 1366348-97-1
2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide

2: potassium carbonate; potassium iodide / 1,2-dimethoxyethane / 16 h / Reflux; Inert atmosphere

With copper(l) iodide; potassium carbonate; potassium iodide; In 1,2-dimethoxyethane;
DOI:10.1016/j.bmc.2012.01.022

Reference yield:

: 637-87-6
1-Chloro-4-iodobenzene

: 1366348-97-1
2-((4-(4-chlorophenyl)-1,4-diazepan-1-yl)methyl)benzo[d]thiazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide

2: potassium carbonate; potassium iodide / 1,2-dimethoxyethane / 16 h / Reflux; Inert atmosphere

With copper(l) iodide; potassium carbonate; potassium iodide; In 1,2-dimethoxyethane;
DOI:10.1016/j.bmc.2012.01.022