3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

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Chemical Name:3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide
CAS No.:1233938-90-3
Molecular Formula:Br*C₂₆H₃₂N₃O₃
Molecular Weight:514.462
Hs Code.:

Synonyms:3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

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Chemical Property of 3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

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Technology Process of 3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

There total 1 articles about 3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1233938-89-0
3-(5-((3R,5R)-1-benzyl-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

: 1233938-90-3
3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

Guidance literature:: With 5% Pd(II)/C(eggshell); hydrogen; In methanol; at 20 ℃; under 760.051 Torr;
DOI:10.1002/ejoc.201000239

Reference yield: 81.0%

: 1233938-90-3
3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

: 3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: With potassium hexafluorophosphate; In water;
DOI:10.1002/ejoc.201000239

Reference yield: 80.0%

: 75-77-4
chloro-trimethyl-silane

: 1233938-90-3
3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide

: 3-(5-((3R,5R)-5-(diphenyl(trimethylsilyloxy)methyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: chloro-trimethyl-silane; 3-(5-((3R,5R)-5-(hydroxydiphenylmethyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium bromide; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 20.25h; Inert atmosphere;

With potassium hexafluorophosphate; In water; for 0.0833333h;
DOI:10.1002/ejoc.201000239