dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester
• CAS No.: 899794-58-2
• Molecular Formula: C₁₈H₂₄O₃S₂
• Molecular Weight: 352.519

Synonyms:dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester

Chemical Property:

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Technology Process of dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester

There total 1 articles about dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

dithiocarbonic acid S-[5,5-dimethyl-4-oxo-1-(2-phenyl[1,3]dioxolan-2-yl)hexyl] ester O-ethyl ester (899794-49-1) → dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester (899794-58-2)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1055/s-2006-926464

Reference yield: 91.0%

dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester (899794-58-2) → dithiocarbonic acid S-(6-tert-butyl-2-phenylpyridin-3-yl) ester O-ethyl ester

Guidance literature:

With air; ammonium acetate; acetic acid; for 1.5h; Heating;

DOI:10.1055/s-2006-926464

Reference yield: 32.0%

1-pentene-3-one ethylene acetal (22515-82-8) + dithiocarbonic acid S-(1-benzoyl-5,5-dimethyl-4-oxohexyl) ester O-ethyl ester (899794-58-2) → dithiocarbonic acid S-[3-benzoyl-1-(2-ethyl-[1,3]dioxolan-2-yl)-7,7-dimethyl-6-oxooctyl] ester O-ethyl ester (540741-14-8)

Guidance literature:

With dilauryl peroxide; In cyclohexane; Heating;

DOI:10.1021/ol0342610

upstream raw materials:

dithiocarbonic acid S-[5,5-dimethyl-4-oxo-1-(2-phenyl[1,3]dioxolan-2-yl)hexyl] ester O-ethyl ester

Downstream raw materials:

dithiocarbonic acid S-[3-benzoyl-1-(2-ethyl-[1,3]dioxolan-2-yl)-7,7-dimethyl-6-oxooctyl] ester O-ethyl ester

2-[2-(2-ethyl-[1,3]dioxolan-2-yl)ethyl]-6,6-dimethyl-1-phenylheptane-1,5-dione

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