Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

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Chemical Name:Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester
CAS No.:118004-31-2
Molecular Formula:C₁₄H₁₃FN₂O₅
Molecular Weight:308.266
Hs Code.:

Synonyms:Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

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Chemical Property of Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

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Technology Process of Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

There total 3 articles about Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 116097-54-2
3-(benzyloxycarbonyloxymethyl)-5-fluorouracil

: 74-88-4
methyl iodide

: 118004-31-2
Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1246/cl.1988.1381

Reference yield:

: 74179-14-9
N¹,N³-bis(hydroxymethyl)-5-fluorouracil

: 118004-31-2
Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / triethylamine / acetonitrile

2: imidazole / acetonitrile

3: 95 percent / ethyldiisopropylamine (EDA) / acetonitrile

With 1H-imidazole; triethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1246/cl.1988.1381

Reference yield:

: 116097-55-3
1,3-bis-(benzyloxycarbonyloxymethyl)-5-fluorouracil

: 118004-31-2
Carbonic acid benzyl ester 5-fluoro-3-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / acetonitrile

2: 95 percent / ethyldiisopropylamine (EDA) / acetonitrile

With 1H-imidazole; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1246/cl.1988.1381