(1,3-bis(diisopropylphosphino)propane)PdCl₂

Base Information

Chemical Name:(1,3-bis(diisopropylphosphino)propane)PdCl₂
CAS No.:134029-36-0
Molecular Formula:C₁₅H₃₄Cl₂P₂Pd
Molecular Weight:453.708
Hs Code.:

(1,3-bis(diisopropylphosphino)propane)PdCl<sub>2</sub>

Synonyms:(1,3-bis(diisopropylphosphino)propane)PdCl₂

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Chemical Property of (1,3-bis(diisopropylphosphino)propane)PdCl₂

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Technology Process of (1,3-bis(diisopropylphosphino)propane)PdCl₂

There total 4 articles about (1,3-bis(diisopropylphosphino)propane)PdCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (CH₂)3(P(CH(CH₃)2)2)2Pd(H)(CO)Pd(P(CH(CH₃)2)2)2(CH₂)3⁽¹⁺⁾*Cl^(1-) = (CH₂)3(P(CH(CH₃)2)2)4Pd₂(CO)(H)(CH₂)3Cl

: 108-90-7
chlorobenzene

: (C₃H₇)2PC₃H₆P(C₃H₇)2PdClCOC₆H₅

: bis(1,3-bis(diisopropylphosphino)propane)(Ph)(Cl)palladium

: 134029-36-0
(1,3-bis(diisopropylphosphino)propane)PdCl₂

Guidance literature:: With triethylamine; In 1,4-dioxane; addn. of a soln. of the palladium complex to a soln. of chlorobenzene and triethylamine, heating at 95°C overnight; (31)P-NMR analysis of the resulting soln.;
DOI:10.1021/om00014a035

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 137203-44-2
Pd(C₆H₅)Cl(P(CH(CH₃)2)2CH₂CH₂CH₂P(CH(CH₃)2)2)

: 134029-36-0
PdCl₂(P(CH(CH₃)2)2CH₂CH₂CH₂P(CH(CH₃)2)2)

: 152850-21-0
(C₆H₅CHCH₂)Pd(P(CH(CH₃)2)2C₃H₆P(CH(CH₃)2)2)

Guidance literature:: In 1,4-dioxane; byproducts: cis-stilbene, trans-stilbene; 140°C;
DOI:10.1021/om00021a021

Reference yield:

: (CH₂)3(P(CH(CH₃)2)2)2Pd(H)(CO)Pd(P(CH(CH₃)2)2)2(CH₂)3⁽¹⁺⁾*Cl^(1-) = (CH₂)3(P(CH(CH₃)2)2)4Pd₂(CO)(H)(CH₂)3Cl

: 100-44-7
benzyl chloride

: 134029-36-0
(1,3-bis(diisopropylphosphino)propane)PdCl₂

: Pd(((CH₃)2CH)2P(CH₂)3P(CH(CH₃)2)2)(CH₂C₆H₅)Cl

Guidance literature:: In acetone; byproducts: toluene, CO; addn. of a soln. of benzyl chloride to the palladium complex, heating at 60°C in a pressure bottle overnight; filtn., drying, evapn. of the soln., extn. of the residue with acetone-d6, elem. anal.;
DOI:10.1021/om00014a035