N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

Base Information

Chemical Name:N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide
CAS No.:133700-44-4
Molecular Formula:C₂₅H₂₆N₂O₇
Molecular Weight:466.491
Hs Code.:

Synonyms:N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

Chemical Property:

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Technology Process of N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

There total 6 articles about N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 133700-29-5
2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethylamine

: 122-04-3
4-nitro-benzoyl chloride

: 133700-44-4
N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

Guidance literature:: With triethylamine; In dichloromethane; for 2h;
DOI:10.1021/jm00110a018

Reference yield:

: 62648-55-9
5-hydroxy-2,3-dimethoxybenzaldehyde

: 133700-44-4
N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 3 h / Heating

2: 87 percent / ammonium acetate, HOAc / 1 h / 70 °C

3: 95 percent / methanol / -10 °C

4: lithium aluminum hydride (LAH) / tetrahydrofuran / 6 h / Heating

5: 90 percent / triethylamine / CH₂Cl₂ / 2 h

With ammonium acetate; lithium aluminium tetrahydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00110a018

Reference yield:

: 93092-16-1
5-(benzyloxy)-2,3-dimethoxybenzaldehyde

: 133700-44-4
N-<2-<2,3-dimethoxy-5-(benzyloxy)phenyl>-2-methoxyethyl>-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / ammonium acetate, HOAc / 1 h / 70 °C

2: 95 percent / methanol / -10 °C

3: lithium aluminum hydride (LAH) / tetrahydrofuran / 6 h / Heating

4: 90 percent / triethylamine / CH₂Cl₂ / 2 h

With ammonium acetate; lithium aluminium tetrahydride; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00110a018