2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

Base Information

Chemical Name:2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine
CAS No.:141690-80-4
Molecular Formula:C₄₄H₃₇N₅O₅S
Molecular Weight:747.874
Hs Code.:

Synonyms:2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

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Chemical Property of 2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

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Technology Process of 2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

There total 4 articles about 2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 51066-54-7
sodium thiobenzoate

: 141690-79-1
6-N,N-Dibenzoyl-9-<2-deoxy-3-O-methanesulphonyl-5-O-(4-monomethoxytrityl)-β-D-threo-pentofuranosyl>adenine

: 141690-80-4
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

: 141690-81-5
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 1.5h; Yields of byproduct given;
DOI:10.1016/S0040-4020(01)88532-X

Reference yield:

: 98-88-4
benzoyl chloride

: 141690-80-4
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 4 h / 0 °C

2: dimethylformamide / 1.5 h / 90 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88532-X

Reference yield:

: 108895-41-6
9-<2-Deoxy-3-O-methanesulphonyl-5-O-(4-monomethoxytrityl)-β-D-threo-pentofuranosyl>adenine

: 141690-80-4
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 4 h / 0 °C

2: dimethylformamide / 1.5 h / 90 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88532-X