2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

Base Information

Chemical Name:2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine
CAS No.:141690-81-5
Molecular Formula:C₅₁H₄₁N₅O₆S
Molecular Weight:851.982
Hs Code.:

Synonyms:2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

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Chemical Property of 2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

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Technology Process of 2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

There total 4 articles about 2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 51066-54-7
sodium thiobenzoate

: 141690-79-1
6-N,N-Dibenzoyl-9-<2-deoxy-3-O-methanesulphonyl-5-O-(4-monomethoxytrityl)-β-D-threo-pentofuranosyl>adenine

: 141690-80-4
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N-benzoyladenosine

: 141690-81-5
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 1.5h; Yields of byproduct given;
DOI:10.1016/S0040-4020(01)88532-X

Reference yield:

: 98-88-4
benzoyl chloride

: 141690-81-5
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 4 h / 0 °C

2: 30 percent / dimethylformamide / 1.5 h / 90 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88532-X

Reference yield:

: 108895-41-6
9-<2-Deoxy-3-O-methanesulphonyl-5-O-(4-monomethoxytrityl)-β-D-threo-pentofuranosyl>adenine

: 141690-81-5
2'-Deoxy-3'-S-thiobenzoyl-5'-O-(4-monomethoxytrityl)-6-N,N-dibenzoyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 4 h / 0 °C

2: 30 percent / dimethylformamide / 1.5 h / 90 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88532-X