C₅₂H₆₅N₅O₂₄

Base Information

• Chemical Name: C₅₂H₆₅N₅O₂₄
• CAS No.: 948995-77-5
• Molecular Formula: C₅₂H₆₅N₅O₂₄
• Molecular Weight: 1144.11
• Mol file: 948995-77-5.mol

Synonyms:C₅₂H₆₅N₅O₂₄

Chemical Property of C₅₂H₆₅N₅O₂₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₂H₆₅N₅O₂₄

There total 11 articles about C₅₂H₆₅N₅O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-[2-(2-azidoethoxy)ethyl]-4-[3,5-dimethyl-4-(4-nitrobenzyloxy)phenyl]-4-oxobutyramide (948995-63-9) + 1-(2-prop-1-ynyl)-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside (182688-43-3) → C52H65N5O24 (948995-77-5)

Guidance literature:

With copper(I) sulfate; copper(II) sulfate; sodium L-ascorbate; at 20 ℃; for 12h;

DOI:10.1021/jo070621b

Reference yield:

4-[3,5-dimethyl-4-(4-nitro-benzyloxy)-phenyl]-4-oxo-butyric acid 2,5-dioxo-pyrrolidin-1-yl ester (948995-62-8) → C52H65N5O24 (948995-77-5)

Guidance literature:

Multi-step reaction with 4 steps

1: CH₂Cl₂ / 3 h / 20 °C

2: pyridine / 12 h / 20 °C

3: 70 percent / NaN₃ / dimethylformamide / 12 h / 20 °C

4: 95 percent / copper sulfate; sodium ascorbate / 12 h / 20 °C

With pyridine; sodium azide; copper(I) sulfate; copper(II) sulfate; sodium L-ascorbate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jo070621b

Reference yield:

C23H28N2O7 → C52H65N5O24 (948995-77-5)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / 12 h / 20 °C

2: 70 percent / NaN₃ / dimethylformamide / 12 h / 20 °C

3: 95 percent / copper sulfate; sodium ascorbate / 12 h / 20 °C

With pyridine; sodium azide; copper(I) sulfate; copper(II) sulfate; sodium L-ascorbate; In N,N-dimethyl-formamide;

DOI:10.1021/jo070621b

upstream raw materials:

N-[2-(2-azidoethoxy)ethyl]-4-[3,5-dimethyl-4-(4-nitrobenzyloxy)phenyl]-4-oxobutyramide

1-(2-prop-1-ynyl)-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

4-[3,5-dimethyl-4-(4-nitro-benzyloxy)-phenyl]-4-oxo-butyric acid 2,5-dioxo-pyrrolidin-1-yl ester

C₁₉H₁₉NO₆

Refernces