α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

Base Information

Chemical Name:α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene
CAS No.:393148-56-6
Molecular Formula:C₅₀H₇₉N₅O₅
Molecular Weight:830.208
Hs Code.:

Synonyms:α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

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Chemical Property of α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

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Technology Process of α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

There total 4 articles about α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 393148-55-5
α-{N-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane}-α'-{bis[2-(2-pyridyl)ethyl]amino}-p-xylene

: 112-67-4
n-hexadecanoyl chloride

: 393148-56-6
α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

: 15496-36-3
bis[2-(2-pyridyl)ethyl]amine

: 393148-56-6
α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / Et₃N / tetrahydrofuran; benzene / 48 h / 40 °C

2: 65 percent / Cs₂CO₃; KJ / acetone / 72 h / 40 °C

3: 64 percent / Et₃N / CH₂Cl₂ / 48 h / 20 °C

With caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetone; benzene;

Reference yield:

: 623-25-6
p-Xylylene dichloride

: 393148-56-6
α-{N-[(N'-1-hexadecanoyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane]}-α'-[bis[2-(2-pyridyl)ethyl]amino]-p-xylene

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / Et₃N / tetrahydrofuran; benzene / 48 h / 40 °C

2: 65 percent / Cs₂CO₃; KJ / acetone / 72 h / 40 °C

3: 64 percent / Et₃N / CH₂Cl₂ / 48 h / 20 °C

With caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetone; benzene;