N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

Base Information

Chemical Name:N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate
CAS No.:107336-58-3
Molecular Formula:C₂₄H₃₁N₃OS₂
Molecular Weight:441.662
Hs Code.:

Synonyms:N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

Chemical Property:

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Technology Process of N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

There total 4 articles about N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 107336-00-5
2-(2-(4-phenyl-1-piperidyl)ethoxy)benzaldehyde

: 556-61-6
methyl thioisocyanate

: 107336-58-3
N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

Guidance literature:: With sodium hydroxide; In ethanol; water;

Reference yield:

: 771-99-3
4-phenylpiperidine

: 107336-58-3
N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃; 2.) 10percent HCl / 1.) DMF, 80 deg C, 22 h; 2.) H₂O, MeOH, 70 deg C, 20 min

2: 1.) NaOH / 1.) EtOH, reflux, 1 h; 2.) reflux, 1.5 h

With hydrogenchloride; sodium hydroxide; potassium carbonate;
DOI:10.1248/cpb.35.2825

Reference yield:

: 103076-66-0
2-(2-chloroethoxy)benzaldehyde ethylene acetal

: 107336-58-3
N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃; 2.) 10percent HCl / 1.) DMF, 80 deg C, 22 h; 2.) H₂O, MeOH, 70 deg C, 20 min

2: 1.) NaOH / 1.) EtOH, reflux, 1 h; 2.) reflux, 1.5 h

With hydrogenchloride; sodium hydroxide; potassium carbonate;
DOI:10.1248/cpb.35.2825