4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

Base Information

Chemical Name:4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate
CAS No.:1411775-04-6
Molecular Formula:CH₂O₂*C₁₄H₁₇N₃O₄
Molecular Weight:337.332
Hs Code.:

Synonyms:4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

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Chemical Property of 4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

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Technology Process of 4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

There total 5 articles about 4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 64-18-6
formic acid

: 1411775-03-5
4-{4-[5-[(dibenzylamino)methyl]-2-oxo-1,3-oxazolidine-3-yl]phenyl}morpholine-3-one

: 1411775-04-6
4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 44h; under 7500.75 Torr;

Reference yield:

: 438056-69-0
4-(4-aminophenyl)morpholin-3-one

: 1411775-04-6
4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol; water / 120 h / 25 °C

2: 1-methyl-pyrrolidin-2-one / toluene / 80 °C / Reflux

3: sodium iodide / acetonitrile / 30 h / Reflux

4: caesium carbonate / 35 h / 80 °C

5: palladium 10% on activated carbon / hydrogen / methanol / 44 h / 20 °C / 7500.75 Torr

With 1-methyl-pyrrolidin-2-one; palladium 10% on activated carbon; caesium carbonate; sodium iodide; hydrogen; In methanol; ethanol; water; toluene; acetonitrile;

Reference yield:

: 1411711-52-8
(dl)-4-[4-[(3-chloro-2-hydroxypropyl)amino]phenyl]-3-morpholinone

: 1411775-04-6
4-{4-[5-aminomethyl-2-oxo-1,3-oxazolidine-3-yl]-phenyl}-morpholine-3-one formate

Guidance literature:: Multi-step reaction with 4 steps

1: 1-methyl-pyrrolidin-2-one / toluene / 80 °C / Reflux

2: sodium iodide / acetonitrile / 30 h / Reflux

3: caesium carbonate / 35 h / 80 °C

4: palladium 10% on activated carbon / hydrogen / methanol / 44 h / 20 °C / 7500.75 Torr

With 1-methyl-pyrrolidin-2-one; palladium 10% on activated carbon; caesium carbonate; sodium iodide; hydrogen; In methanol; toluene; acetonitrile;