Technology Process of C30H24FN3O2S
There total 9 articles about C30H24FN3O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
methanol; ethyl acetate;
at 20 ℃;
for 7h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: tetrahydrofuran / 1 h / Cooling with ice
2.1: sodium hydroxide; water / methanol / 0.5 h / Cooling with ice
3.1: sulfuric acid / 4 h / Cooling with ice
4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
5.1: borane-THF / tetrahydrofuran / 3 h / 20 °C / Cooling with ice
5.2: 0.25 h / 20 °C / Cooling with ice
6.1: acetone / 1.5 h / Cooling with ice
7.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C / Cooling with ice
8.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 7 h / 20 °C
With
borane-THF; oxalyl dichloride; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; sulfuric acid; water; hydrogen; sodium hydroxide;
palladium 10% on activated carbon; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetone / 1.5 h / Cooling with ice
2: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C / Cooling with ice
3: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 7 h / 20 °C
With
1-chloro-1-(dimethylamino)-2-methyl-1-propene; hydrogen;
palladium 10% on activated carbon;
In
methanol; dichloromethane; ethyl acetate; acetone;
