N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

Base Information

Chemical Name:N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester
CAS No.:108826-71-7
Molecular Formula:C₄₃H₆₅N₅O₉Si
Molecular Weight:824.103
Hs Code.:

Synonyms:N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

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Chemical Property of N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

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Technology Process of N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

There total 4 articles about N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 79385-71-0
N^ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester hydrochloride

: 2279-15-4
N-(benzyloxycarbonyl)-D-tryptophan

: 108826-71-7
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 4 ℃; for 16h;

Reference yield:

: 3338-34-9
Z-Lys(-Boc)-Osu

: 108826-71-7
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NEt₃ / acetonitrile / 6 h / 20 °C

2: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

3: 61 percent / 1.) HOBt, DCC; 2.) Et₃N / dimethylformamide / 16 h / 4 °C

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 79385-70-9
H-Thr(Bu^t)-OTmse

: 108826-71-7
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NEt₃ / acetonitrile / 6 h / 20 °C

2: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

3: 61 percent / 1.) HOBt, DCC; 2.) Et₃N / dimethylformamide / 16 h / 4 °C

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;