N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

Base Information

Chemical Name:N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine
CAS No.:108826-72-8
Molecular Formula:C₃₈H₅₃N₅O₉
Molecular Weight:723.867
Hs Code.:

Synonyms:N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

Chemical Property:

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Technology Process of N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

There total 5 articles about N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108826-71-7
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine 2-trimethylsilylethyl ester

: 108826-72-8
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

Guidance literature:: With tetraethylammonium fluoride; In N,N-dimethyl-formamide; at 30 ℃; for 0.5h;

Reference yield:

: 3338-34-9
Z-Lys(-Boc)-Osu

: 108826-72-8
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NEt₃ / acetonitrile / 6 h / 20 °C

2: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

3: 61 percent / 1.) HOBt, DCC; 2.) Et₃N / dimethylformamide / 16 h / 4 °C

4: 93 percent / Et₄NF / dimethylformamide / 0.5 h / 30 °C

With hydrogen; tetraethylammonium fluoride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 79385-70-9
H-Thr(Bu^t)-OTmse

: 108826-72-8
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NEt₃ / acetonitrile / 6 h / 20 °C

2: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

3: 61 percent / 1.) HOBt, DCC; 2.) Et₃N / dimethylformamide / 16 h / 4 °C

4: 93 percent / Et₄NF / dimethylformamide / 0.5 h / 30 °C

With hydrogen; tetraethylammonium fluoride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;