4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

Base Information

Chemical Name:4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone
CAS No.:1381791-46-3
Molecular Formula:C₂₁H₁₇ClF₃NO₃
Molecular Weight:423.819
Hs Code.:

Synonyms:4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

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Chemical Property of 4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

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Technology Process of 4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

There total 3 articles about 4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74-96-4
ethyl bromide

: 1381792-12-6
4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-2(1H)-pyridinone

: 1381791-46-3
4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

Guidance literature:: ethyl bromide; 4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-2(1H)-pyridinone; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 80 ℃; for 1h;

With methanol; In N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1369255-78-6
1-chloro-4-(4-(chloromethyl)phenoxy)-2-(trifluoromethyl)benzene

: 1381791-46-3
4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 80 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1369257-58-8
(4-(4-chloro-3-(trifluoromethyl)phenoxy)phenyl)methanol

: 1381791-46-3
4-{[(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)methyl]oxy}-1-ethyl-2(1H)-pyridinone

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 1 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 60 °C

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 80 °C

With thionyl chloride; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil;