allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

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Chemical Name:allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate
CAS No.:777062-45-0
Molecular Formula:C₄₈H₅₄ClN₄O₆PSi
Molecular Weight:877.492
Hs Code.:

allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

Synonyms:allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

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Chemical Property of allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

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Technology Process of allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

There total 1 articles about allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 777062-44-9
(4-{[(2R,3S)-1-[2-(allyloxy)-2-oxo-1-(triphenylphosphoranilidene)ethyl]-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4-oxoazetidin-2-yl]acetyl}-2-chlorophenyl)acetic acid

: 13400-46-9
4-aminomethyl-1H-imidazole

: 777062-45-0
allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 2.58333h;

Reference yield: 83.0%

: 75-77-4
chloro-trimethyl-silane

: 777062-45-0
allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate

: 777062-47-2
allyl 5-{[({4-[((2R,3S)-1-[2-(allyloxy)-2-oxo-1-(triphenylphosphoranilidene)ethyl]-4-oxo-3-{(1R)-1-[(trimethylsilyl)oxy]ethyl}azetidin-2-yl)acetyl]-2-chlorophenyl}acetyl)amino]methyl}-1H-imidazole-1-carboxylate

Guidance literature:: allyl {[(2R,3S)-3-((1R)-1-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-2-[2-(3-chloro-4-{2-[(1H-imidazol-5-ylmethyl)amino]-2-oxoethyl}phenyl)-2-oxoethyl]-4-oxoazetidin-1-yl]}(triphenylphosphoranilidene)acetate; Allyl chloroformate; With pyridine; dmap; at 0 ℃; for 0.333333h;

With trifluoroacetic acid; at 0 ℃; for 0.583333h;

chloro-trimethyl-silane; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;