2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

Base Information

Chemical Name:2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride
CAS No.:1239964-48-7
Molecular Formula:C₁₁H₁₅ClN₂O₂*ClH
Molecular Weight:279.166
Hs Code.:

Synonyms:2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

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Chemical Property of 2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

Chemical Property:

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Technology Process of 2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

There total 5 articles about 2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1239964-47-6
tert-butyl 2-(2-(4-chloro-3-methoxyphenyl)-2-methylpropanoyl)hydrazine carboxylate

: 1239964-48-7
2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; ethyl acetate; at 0 - 20 ℃; for 18h;

Reference yield:

: 850564-15-7
2-(4-Chloro-3-methoxy-phenyl)-2-methyl-propionitrile

: 1239964-48-7
2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 20 h / Reflux

2: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 15 h

3: hydrogenchloride / ethyl acetate; diethyl ether / 18 h / 0 - 20 °C

With hydrogenchloride; sulfuric acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; ethyl acetate;

Reference yield:

: 1239963-78-0
2-(4-chloro-3-methoxyphenyl)-2-methylpropanoic acid

: 1239964-48-7
2-(4-chloro-3-methoxyphenyl)-2-methylpropanehydrazide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 15 h

2: hydrogenchloride / ethyl acetate; diethyl ether / 18 h / 0 - 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; ethyl acetate;