Technology Process of C22H17BrN4S
There total 3 articles about C22H17BrN4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
N,N-dimethyl-formamide; acetone;
at 20 ℃;
for 14h;
DOI:10.1007/s11164-012-0538-5
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / acetone / 20 °C
2: trichlorophosphate / 2 h / Reflux
3: acetic acid / ethanol / 1 h / Reflux
4: manganese(IV) oxide / N,N-dimethyl-formamide; acetone / 14 h / 20 °C
With
manganese(IV) oxide; acetic acid; potassium hydroxide; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1007/s11164-012-0538-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate / 2 h / Reflux
2: acetic acid / ethanol / 1 h / Reflux
3: manganese(IV) oxide / N,N-dimethyl-formamide; acetone / 14 h / 20 °C
With
manganese(IV) oxide; acetic acid; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1007/s11164-012-0538-5