(2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

Base Information

Chemical Name:(2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate
CAS No.:1404217-34-0
Molecular Formula:C₃₅H₃₉NO₆Si
Molecular Weight:597.783
Hs Code.:

Synonyms:(2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

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Chemical Property of (2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

Chemical Property:

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Technology Process of (2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

There total 4 articles about (2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404217-33-9
benzyl N-[(2R,3S)-1-[(tert-butyldiphenylsilyl)oxy]-3,4-dihydroxybutan-2-yl]carbamate

: 98-88-4
benzoyl chloride

: 1404217-34-0
(2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

Guidance literature:: With pyridine; In dichloromethane; for 0.5h; Cooling with acetone-dry ice;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1404217-34-0
(2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / Cooling with ice

2: sodium hydrogencarbonate / water; tetrahydrofuran / 48 h

3: acetic acid / water; tetrahydrofuran / 5 h / 50 °C

4: pyridine / dichloromethane / 0.5 h / Cooling with acetone-dry ice

With pyridine; 1H-imidazole; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 177186-42-4
(2S,3R)-3-amino-4-tert-butyldiphenylsilyloxy-1,2-isopropylidenedioxy-butane

: 1404217-34-0
(2S,3R)-3-{[(benzyloxy)carbonyl]amino}-4-[(tert-butyldiphenylsilyl)oxy]-2-hydroxybutyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water; tetrahydrofuran / 48 h

2: acetic acid / water; tetrahydrofuran / 5 h / 50 °C

3: pyridine / dichloromethane / 0.5 h / Cooling with acetone-dry ice

With pyridine; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; dichloromethane; water;