C₂₄H₃₄F₂N₄O

Base Information

Chemical Name:C₂₄H₃₄F₂N₄O
CAS No.:960391-46-2
Molecular Formula:C₂₄H₃₄F₂N₄O
Molecular Weight:432.557
Hs Code.:

C<sub>24</sub>H<sub>34</sub>F<sub>2</sub>N<sub>4</sub>O

Synonyms:C₂₄H₃₄F₂N₄O

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Chemical Property of C₂₄H₃₄F₂N₄O

Chemical Property:

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Technology Process of C₂₄H₃₄F₂N₄O

There total 8 articles about C₂₄H₃₄F₂N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960391-36-0
tert-butyl [1-({2-tert-butyl-1-[(4,4-difluorocyclohexyl)methyl]-1H-benzimidazol-5-yl}carbonyl)piperidin-4-yl]carbamate

: 960391-46-2
C₂₄H₃₄F₂N₄O

Guidance literature:: tert-butyl [1-({2-tert-butyl-1-[(4,4-difluorocyclohexyl)methyl]-1H-benzimidazol-5-yl}carbonyl)piperidin-4-yl]carbamate; With hydrogenchloride; acetic acid; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 809273-66-3
methyl {[(4,4-difluorocyclohexyl)methanol]amino}-3-nitrobenzoate

: 960391-46-2
C₂₄H₃₄F₂N₄O

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 48 h / 20 °C / 2585.81 Torr

2.1: dmap / dichloromethane / 4 h / 20 °C

3.1: acetic acid / 3 h / 150 °C / Microwave irradiation

4.1: lithium hydroxide; water / 1,4-dioxane / 3 h / 75 °C

4.2: pH 5 - 6

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.1: hydrogenchloride; acetic acid / 1 h / 20 °C

With hydrogenchloride; dmap; lithium hydroxide; water; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 809273-65-2
(4,4-difluorocyclohexane)methylamine hydrochloride

: 960391-46-2
C₂₄H₃₄F₂N₄O

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 75 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 48 h / 20 °C / 2585.81 Torr

3.1: dmap / dichloromethane / 4 h / 20 °C

4.1: acetic acid / 3 h / 150 °C / Microwave irradiation

5.1: lithium hydroxide; water / 1,4-dioxane / 3 h / 75 °C

5.2: pH 5 - 6

6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

7.1: hydrogenchloride; acetic acid / 1 h / 20 °C

With hydrogenchloride; dmap; lithium hydroxide; water; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;