(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE

Base Information

Chemical Name:(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE
CAS No.:42287-48-9
Molecular Formula:C₁₆H₁₉N
Molecular Weight:225.334
Hs Code.:
Mol file:42287-48-9.mol

Synonyms:Benzenemethanamine,a-methyl-N-(1-phenylethyl)-,(R*,R*)-(?à)-; Dibenzylamine, a,a'-dimethyl-, (?à)- (8CI); Benzenemethanamine, a-methyl-N-(1-phenylethyl)-,(R*,R*)-

Suppliers and Price of (R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE 95.00%
1G
$ 641.04

Total 4 raw suppliers

Chemical Property of (R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE

Chemical Property:

Melting Point:~260 °C
PSA：12.03000
LogP:5.29130

Purity/Quality:

98%min ^*data from raw suppliers

(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE

There total 89 articles about (R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 40636-57-5
(αS)-α-methyl-N-(1-phenylethylidene)benzenemethanamine

: 21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1,10024-74-5
(1S,1'S)-bis(1-phenylethyl)amine

Guidance literature:: With N,N'-dimethyl-(R)-1,1'-binaphthyldiamine-bis-2-pyridinecarboxyamide; trichlorosilane; In dichloromethane; at 0 ℃; for 12h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol900945h

Reference yield: 91.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 98-86-2
acetophenone

: 21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1,10024-74-5
(1S,1'S)-bis(1-phenylethyl)amine

Guidance literature:: (S)-1-phenyl-ethylamine; acetophenone; With tris(pentafluorophenyl)borate; In toluene; at 60 ℃; for 8h; Molecular sieve;

With ammonia borane; In toluene; at 0 ℃; for 12h; Solvent; Temperature; diastereoselective reaction; Molecular sieve;
DOI:10.1021/acs.joc.8b01362

Reference yield: 88.0%

: 98-86-2
acetophenone

: 10024-74-5,21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1
(R,R)-N,N-bis-(1-phenylethyl)amine

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; ammonium acetate; hydrogen; 2-((11bS)-2,6-di(naphthalen-1-yl)dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)-1,2,3,4-tetrahydroisoquinoline; toluene-4-sulfonic acid; In methanol; dichloromethane; at 80 ℃; for 24h; under 45603.1 Torr; Reagent/catalyst; stereoselective reaction; Catalytic behavior; Autoclave;
DOI:10.1002/anie.202112671