N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide

Base Information

• Chemical Name: N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide
• CAS No.: 122702-25-4
• Molecular Formula: C₃₃H₄₀N₄O₆S
• Molecular Weight: 620.77
• Mol file: 122702-25-4.mol

Synonyms:N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide

Chemical Property of N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide

There total 7 articles about N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-Tyr-NH2 (4985-46-0) → N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide (122702-25-4)

Guidance literature:

Multi-step reaction with 3 steps

1: ethyl acetate; CHCl₃

2: HBr; acetic acid

3: ethyl acetate; DMF

With chloroform; hydrogen bromide; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1039/jr9580004541

Reference yield:

S-Benzyl-N-benzyloxycarbonyl-L-cysteinylazid → N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide (122702-25-4)

Guidance literature:

Multi-step reaction with 4 steps

1: ethyl acetate; CHCl₃

2: methanol. NH₃

3: HBr; acetic acid

4: ethyl acetate; DMF

With chloroform; ammonia; hydrogen bromide; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1039/jr9580004541

Reference yield:

Z-Leu-OH (2018-66-8) → N-benzyloxycarbonyl-leucyl=>S-benzyl-cysteinyl=>tyrosine amide (122702-25-4)

Guidance literature:

With chloroform; chloroformic acid ethyl ester; triethylamine; N-benzyloxycarbonyl-L-leucyl=>S-benzyl-L-cysteinyl=>L-tyrosine amide; anschliessend Behandeln mit N-<S-Benzyl-L-cysteinyl>-L-tyrosin-amid in DMF;

DOI:10.1039/jr9580004541

upstream raw materials:

Z-Leu-OH

(S)-benzyl (1-azido-4-methyl-1-oxopentan-2-yl)carbamate

N-(S-benzyl-L-cysteinyl)-L-tyrosine amide

L-Tyr-OMe