Technology Process of C49H39Cl3N8O13P2
There total 5 articles about C49H39Cl3N8O13P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N1,N1,N3,N3-tetrametylquanidium salt of 2-pyridinecarboxaldehyde oxim;
In
1,4-dioxane; water;
for 16h;
Ambient temperature;
DOI:10.1021/jo00146a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 75 percent / 8-quinolinesulfonyl tetrazolide / pyridine / 2 h / Ambient temperature
2: 81 percent / 8-quinolinesulfonyl tetrazolide / pyridine / 2 h
3: N1,N1,N3,N3-tetramethylguanidium salt of pyridine-2-carboaldoxime / dioxane; H2O / 16 h / Ambient temperature
With
N1,N1,N3,N3-tetrametylquanidium salt of 2-pyridinecarboxaldehyde oxim; 8-quinolinesulphonyl tetrazolide;
In
1,4-dioxane; pyridine; water;
DOI:10.1021/jo00146a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 75 percent / 8-quinolinesulfonyl tetrazolide / pyridine / 2 h / Ambient temperature
2: 81 percent / 8-quinolinesulfonyl tetrazolide / pyridine / 2 h
3: N1,N1,N3,N3-tetramethylguanidium salt of pyridine-2-carboaldoxime / dioxane; H2O / 16 h / Ambient temperature
With
N1,N1,N3,N3-tetrametylquanidium salt of 2-pyridinecarboxaldehyde oxim; 8-quinolinesulphonyl tetrazolide;
In
1,4-dioxane; pyridine; water;
DOI:10.1021/jo00146a022