Technology Process of C24H32N8O7S3
There total 10 articles about C24H32N8O7S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: H2 / Pd/CaCO3/Pb / tetrahydrofuran
2.1: NaN3; nBu4NI / dimethylformamide
3.1: 85 percent / nBu4NI; K2CO3 / acetonitrile
4.1: Me3P; H2O / tetrahydrofuran
5.1: iPr2NEt / acetonitrile
6.1: pyridine; DMAP / CH2Cl2
7.1: NaN3 / dimethylformamide / -15 °C
8.1: 74 percent / (NH4)2Ce(NO3)6 / CH2Cl2; 2-methyl-propan-2-ol
9.1: tBuOK
9.2: 70 percent / (Me3Si)2NH
10.1: 95 percent / H2O / acetonitrile / 70 °C
With
pyridine; dmap; sodium azide; ammonium cerium(IV) nitrate; potassium tert-butylate; water; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trimethylphosphane;
Lindlar's catalyst;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja0608545
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 85 percent / nBu4NI; K2CO3 / acetonitrile
2.1: Me3P; H2O / tetrahydrofuran
3.1: iPr2NEt / acetonitrile
4.1: pyridine; DMAP / CH2Cl2
5.1: NaN3 / dimethylformamide / -15 °C
6.1: 74 percent / (NH4)2Ce(NO3)6 / CH2Cl2; 2-methyl-propan-2-ol
7.1: tBuOK
7.2: 70 percent / (Me3Si)2NH
8.1: 95 percent / H2O / acetonitrile / 70 °C
With
pyridine; dmap; sodium azide; ammonium cerium(IV) nitrate; potassium tert-butylate; water; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trimethylphosphane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja0608545