1--1-cyclohexanol

Base Information

• Chemical Name: 1--1-cyclohexanol
• CAS No.: 15015-46-0
• Molecular Formula: C₁₉H₂₂O₂
• Molecular Weight: 282.382

Synonyms:1--1-cyclohexanol

Chemical Property of 1--1-cyclohexanol

Chemical Property:

Purity/Quality:

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Technology Process of 1--1-cyclohexanol

There total 13 articles about 1--1-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tetraphenylethane-1,2-diol (464-72-2) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → benzophenone (119-61-9) + 1--1-cyclohexanol (15015-46-0)

Guidance literature:

With titanium(IV) tetrabutoxide; triethylsilyl chloride; In dichloromethane; at 20 ℃;

DOI:10.1002/adsc.201200358

Reference yield: 47.0%

benzophenone (119-61-9) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1--1-cyclohexanol (15015-46-0)

Guidance literature:

With lanthanum; iodine; In tetrahydrofuran; at 25 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.tet.2014.12.089

Reference yield: 45.0%

benzophenone (119-61-9) + cyclohexane-1,2-epoxide (286-20-4) → 1--1-cyclohexanol (15015-46-0)

Guidance literature:

With lanthanum; iodine; In tetrahydrofuran; for 3h; Inert atmosphere;

DOI:10.1016/j.tet.2014.12.089

upstream raw materials:

ethylmagnesium iodide

tetraphenylethane-1,2-diol

methyl 1-hydroxycyclohexanecarboxylate

1-amino-1-cyclohexanecarboxylic acid ethyl ester

Downstream raw materials:

phenyl-(1-phenyl-cyclohexyl)-ketone

2,2-diphenylcycloheptanone

1,1-Diphenylmethanol

cyclohexanone

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