(4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid

Base Information Edit

Chemical Name:(4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid
CAS No.:87637-48-7
Molecular Formula:C₂₀H₂₀N₂O₅
Molecular Weight:368.389
Hs Code.:
Mol file:87637-48-7.mol

Synonyms:(4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid

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Chemical Property of (4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid Edit

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Technology Process of (4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid

There total 2 articles about (4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 26339-42-4,26340-00-1
(4S,5R)-1,3-dibenzyl-1H-furo[3,4-d]imidazole-2,4,6-trione

: 83889-77-4
(4S,5R)-1,3-bisbenzyl-2-oxo-5-(methoxycarbonyl)imidazolidin-4-carboxylic acid

: 87637-48-7
(4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid

Guidance literature:: With 8-dihydroquinidyl-phenanthrene; In diethyl ether; at -40 ℃; for 28h; Further Variations:; Reagents; Temperatures; Product distribution;
DOI:10.1055/s-2001-16748

Reference yield:

: 51591-75-4,634188-82-2
cis-1,3-dibenzyl-2-oxoimidazolidine-4,5-dicarboxylic acid

: 87637-48-7
(4R,5S)-1,3-dibenzyl-5-(methoxycarbonyl)-2-oxo-imidazolidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Amberlyst 15 / toluene / 3 h / Reflux

2: 3-(3,5-bis(trifluoromethyl)phenylamino)-4-((1R,2R)-1-(4-nitrophenyl)-2-(pyrrolidin-1-yl)-3-(trityloxy)propylamino)cyclobut-3-ene-1,2-dione / tert-butyl methyl ether / 18 h / 25 °C

With 3-(3,5-bis(trifluoromethyl)phenylamino)-4-((1R,2R)-1-(4-nitrophenyl)-2-(pyrrolidin-1-yl)-3-(trityloxy)propylamino)cyclobut-3-ene-1,2-dione; In tert-butyl methyl ether; toluene;