tribenzyl tetrathiophosphate

Base Information

• Chemical Name: tribenzyl tetrathiophosphate
• CAS No.: 3248-42-8
• Molecular Formula: C₂₁H₂₁PS₄
• Molecular Weight: 432.635
• Mol file: 3248-42-8.mol

Synonyms:tribenzyl tetrathiophosphate

Chemical Property of tribenzyl tetrathiophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tribenzyl tetrathiophosphate

There total 4 articles about tribenzyl tetrathiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

benzyl chloride (100-44-7) → tribenzyl tetrathiophosphate (3248-42-8)

Guidance literature:

With tetraphosphorus decasulfide; potassium carbonate; In acetonitrile; at 50 - 60 ℃; for 2h;

DOI:10.1080/10426509808045492

Reference yield:

phenylmethanethiol (100-53-8) → tribenzyl tetrathiophosphate (3248-42-8)

Guidance literature:

With tetraphosphorus decasulfide; xylene;

Reference yield:

S,S-dibenzyl phenyldithiophosphinite (63832-88-2) → S,S-dibenzyl phenyltrithiophosphonate (138123-45-2) + tribenzyl tetrathiophosphate (3248-42-8) + benzylphenyl-S-benzyldithiophosphinate (138123-46-3)

Guidance literature:

With oxygen; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1007/BF00960423

upstream raw materials:

phenylmethanethiol

S,S-dibenzyl phenyldithiophosphinite

benzyl chloride

tetrachloromethane