1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

Base Information

Chemical Name:1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine
CAS No.:1352234-72-0
Molecular Formula:C₂₄H₂₈N₂O₇
Molecular Weight:456.496
Hs Code.:

Synonyms:1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

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Chemical Property of 1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

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Technology Process of 1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

There total 16 articles about 1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1352234-71-9
C₂₁H₂₆O₇

: 65-71-4,28806-14-6,691841-57-3
thymin

: 1352234-72-0
1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

Guidance literature:: C₂₁H₂₆O₇; thymin; With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 83 ℃;

With tetrabutyl ammonium fluoride; In tetrahydrofuran;

Reference yield:

: C₂₅H₂₇F₃N₂O₉S

: 1352234-72-0
1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/jo401166q

Reference yield:

: 1352234-69-5
1,2-O-isopropylidene-3-keto-5-O-benzyl-6-deoxy-6-C-vinyl-α-D-galactofuranose

: 1352234-72-0
1-(2-O-acetyl-5-O-benzyl-6-deoxy-3,6-C-divinyl-β-D-gulofuranosyl)thymine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 °C

2.1: dowex 50W₈X / 1,4-dioxane; water / 50 °C

2.2: 0 - 25 °C

3.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0 - 83 °C

With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile;