4-Methyl-N,N-diphenylbenzamide

Base Information

Chemical Name:4-Methyl-N,N-diphenylbenzamide
CAS No.:40686-26-8
Molecular Formula:C₂₀H₁₇NO
Molecular Weight:287.361
Hs Code.:

Synonyms:4-Methyl-N,N-diphenylbenzamide

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Chemical Property of 4-Methyl-N,N-diphenylbenzamide

Chemical Property:

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Technology Process of 4-Methyl-N,N-diphenylbenzamide

There total 12 articles about 4-Methyl-N,N-diphenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 591-50-4
iodobenzene

: 6833-18-7
4-methyl-N-phenylbenzamide

: 40686-26-8
4-Methyl-N,N-diphenylbenzamide

Guidance literature:: With caesium carbonate; copper(ll) bromide; N,N`-dimethylethylenediamine; In toluene; at 130 ℃; for 24h;
DOI:10.1002/cjoc.201200701

Reference yield: 86.0%

: 6833-18-7
4-methyl-N-phenylbenzamide

: 62-53-3
aniline

: 40686-26-8
4-Methyl-N,N-diphenylbenzamide

Guidance literature:: With trifluoromethylsulfonic anhydride; triethylamine; Triphenylphosphine oxide; In 1,2-dichloro-ethane; at 25 ℃; for 0.25h;
DOI:10.1021/jo00266a028

Reference yield: 44.0%

: 624-31-7
4-tolyl iodide

: potassium 2-(diphenylamino)-2-oxoacetate

: 40686-26-8
4-Methyl-N,N-diphenylbenzamide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium dihydrogenphosphate; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In N,N-dimethyl acetamide; at 25 ℃; for 20h; chemoselective reaction; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1002/chem.201502286