7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

Base Information

Chemical Name:7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide
CAS No.:1026499-15-9
Molecular Formula:C₁₆H₂₂BrN₃O₆S
Molecular Weight:464.337
Hs Code.:

Synonyms:7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

Suppliers and Price of 7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

There total 2 articles about 7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-64-8
1,3-dibromo-propane

: 312283-45-7
N-(2-nitrobenzenesulfonyl)-N'-(allyloxycarbonyl)-1,3-diaminopropane

: 1026499-15-9
7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h;
DOI:10.1016/j.tet.2006.06.051

Reference yield:

: 240423-09-0
N-(6-aminopropyl)-2-nitrobenzenesulfonamide

: 1026499-15-9
7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

2: 90 percent / Cs₂CO₃ / dimethylformamide / 0.5 h / 50 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2006.06.051

Reference yield:

: 1026499-15-9
7-(allyloxycarbonylamino)-4-(2-nitrobenzenesulfonyl)-4-azaheptan-1-yl bromide

: 437718-36-0
N-[N^α-(tert-butoxycarbonyl)-L-asparaginyl]-N'-(2-nitrobenzenesulfonyl)-1,5-diaminopentane

: 1026386-49-1
{3-[{3-[[5-(2-tert-butoxycarbonylamino-3-carbamoyl-propionylamino)-pentyl]-(2-nitro-benzenesulfonyl)-amino]-propyl}-(2-nitro-benzenesulfonyl)-amino]-propyl}-carbamic acid allyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 1h;
DOI:10.1016/j.tet.2006.06.051