C₈H₇FO₃

Base Information

Chemical Name:C₈H₇FO₃
CAS No.:1417996-86-1
Molecular Formula:C₈H₇FO₃
Molecular Weight:170.14
Hs Code.:

C<sub>8</sub>H<sub>7</sub>FO<sub>3</sub>

Synonyms:C₈H₇FO₃

Suppliers and Price of C₈H₇FO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₈H₇FO₃

Chemical Property:

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Technology Process of C₈H₇FO₃

There total 1 articles about C₈H₇FO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 167683-93-4
2-fluoro-4-methoxy-phenol

: 1417996-86-1
C₈H₇FO₃

Guidance literature:: With triethylamine; magnesium chloride; In acetonitrile; for 8h; Inert atmosphere; Reflux;
DOI:10.1021/ol501496n

Reference yield: 71.0%

: 1417996-86-1
C₈H₇FO₃

: 106-95-6
allyl bromide

: 1615214-13-5
C₁₁H₁₁FO₃

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 10h; Inert atmosphere; Reflux;
DOI:10.1021/ol501496n

Reference yield:

: 1417996-86-1
C₈H₇FO₃

: 1615224-45-7
C₂₇H₃₀BF₃N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / tetrahydrofuran / 10 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / 1,2-dichloro-ethane / 4 h / Inert atmosphere; Reflux

2.2: 2 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 8 h / 20 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol / 8 h / Inert atmosphere; Reflux

5.1: sodium hypochlorite / aq. phosphate buffer; N,N-dimethyl-formamide / 0.5 h / pH 7.4

With sodium hypochlorite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; aq. phosphate buffer; ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ol501496n