C₂₁H₂₂N₂O₅

Base Information

Chemical Name:C₂₁H₂₂N₂O₅
CAS No.:1363373-78-7
Molecular Formula:C₂₁H₂₂N₂O₅
Molecular Weight:382.416
Hs Code.:

C<sub>21</sub>H<sub>22</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₁H₂₂N₂O₅

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Chemical Property of C₂₁H₂₂N₂O₅

Chemical Property:

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Technology Process of C₂₁H₂₂N₂O₅

There total 4 articles about C₂₁H₂₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1363373-78-7
C₂₁H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 2 h / 20 °C

1.2: 20 h / Reflux; Inert atmosphere

2.1: acetic acid / tetrahydrofuran / 2.33 h / 0 - 20 °C / molecular sieves 4?; Inert atmosphere

2.2: 48 h / 20 °C

2.3: pH 10

3.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 36 h / 20 °C / Sealed vessel; Inert atmosphere

4.1: sodium hydroxide; methanol / 1 h / 20 °C / Reflux

4.2: pH 2

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With methanol; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;

Reference yield:

: 17061-85-7
1-nitro-4-(prop-2-ynyloxy)benzene

: 1363373-78-7
C₂₁H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / tetrahydrofuran / 2.33 h / 0 - 20 °C / molecular sieves 4?; Inert atmosphere

1.2: 48 h / 20 °C

1.3: pH 10

2.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 36 h / 20 °C / Sealed vessel; Inert atmosphere

3.1: sodium hydroxide; methanol / 1 h / 20 °C / Reflux

3.2: pH 2

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With methanol; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 26557-78-8
4-(prop-2-ynyloxy)aniline

: 1363373-78-7
C₂₁H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 36 h / 20 °C / Sealed vessel; Inert atmosphere

2.1: sodium hydroxide; methanol / 1 h / 20 °C / Reflux

2.2: pH 2

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With methanol; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide;