Technology Process of C19H13F4NO3
There total 6 articles about C19H13F4NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; pyridine N-oxide; oxygen; copper diacetate;
In
dichloromethane;
at 20 ℃;
for 38h;
Molecular sieve;
- Guidance literature:
-
With
pyridine; pyridine N-oxide; copper diacetate;
at 20 ℃;
for 38h;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-Bromosuccinimide / acetonitrile / 12 h / 70 - 85 °C / Darkness
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; 1,2-dimethoxyethane / 10 h / 90 - 100 °C / Inert atmosphere
3: hydrogen bromide / water / 7 h / 100 °C
4: copper diacetate; pyridine N-oxide; pyridine; oxygen / dichloromethane / 38 h / 20 °C / Molecular sieve
With
pyridine; pyridine N-oxide; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); hydrogen bromide; oxygen; copper diacetate; potassium carbonate;
In
1,2-dimethoxyethane; dichloromethane; water; acetonitrile;