4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide

Base Information

Chemical Name:4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide
CAS No.:328552-93-8
Molecular Formula:C8H11 N3 O
Molecular Weight:165.195
Hs Code.:2925290090
DSSTox Substance ID:DTXSID10695340
Nikkaji Number:J1.679.000A
Mol file:328552-93-8.mol

Synonyms:328552-93-8;4-(Aminomethyl)-N'-hydroxybenzene-1-carboximidamide;4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide;4-(Aminomethyl)benzamideoxime;DTXSID10695340;AKOS017404984

Suppliers and Price of 4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide

Chemical Property:

Boiling Point:374.9°Cat760mmHg
PKA:15.07±0.50(Predicted)
Flash Point:180.5°C
PSA：84.63000
Density:1.28g/cm³
LogP:1.64040
XLogP3:-0.1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:165.090211983
Heavy Atom Count:12
Complexity:162

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1CN)C(=NO)N

Technology Process of 4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide

There total 3 articles about 4-(Aminomethyl)-N-hydroxy-benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 10406-25-4
4-aminobenzyl cyanide

: 328552-93-8
4-(aminomethyl)-N-hydroxybenzene-1-carboximidamide

Guidance literature:: With 4-methyl-morpholine; hydroxylamine hydrochloride; In methanol; at 20 ℃; for 72h;
DOI:10.1016/S0960-894X(02)00010-0

Reference yield:

: 84466-87-5
4-(azidomethyl)benzonitrile

: 328552-93-8
4-(aminomethyl)-N-hydroxybenzene-1-carboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂ / Pd/C / ethyl acetate / 11 h / 2327.17 Torr

2: 89 percent / NH₂OH*HCl; NMM / methanol / 72 h / 20 °C

With 4-methyl-morpholine; hydroxylamine hydrochloride; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1016/S0960-894X(02)00010-0

Reference yield:

: 17201-43-3
4-cyanobenzyl bromide

: 328552-93-8
4-(aminomethyl)-N-hydroxybenzene-1-carboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

2: 93 percent / H₂ / Pd/C / ethyl acetate / 11 h / 2327.17 Torr

3: 89 percent / NH₂OH*HCl; NMM / methanol / 72 h / 20 °C

With 4-methyl-morpholine; sodium azide; hydroxylamine hydrochloride; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00010-0