4-AMINOMETHYL BENZAMIDINE DIHYDROCHLORIDE

Base Information

• Chemical Name: 4-AMINOMETHYL BENZAMIDINE DIHYDROCHLORIDE
• CAS No.: 32797-61-8
• Molecular Formula: C8H11 N3
• Molecular Weight: 149.195
• Hs Code.: 2925290090
• Mol file: 32797-61-8.mol

Synonyms:p-Toluamidine,a-amino- (8CI);4-(Aminomethyl)benzenecarboximidamide; 4-Aminomethylbenzamidine;p-Aminomethylbenzamidine

Chemical Property of 4-AMINOMETHYL BENZAMIDINE DIHYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 0.00309mmHg at 25°C
• Boiling Point: 283.8°C at 760 mmHg
• Flash Point: 125.5°C
• PSA: 75.89000
• LogP: 3.53370

Purity/Quality:

97% ^*data from raw suppliers

4-Aminomethyl benzamidine dihydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AMINOMETHYL BENZAMIDINE DIHYDROCHLORIDE

There total 11 articles about 4-AMINOMETHYL BENZAMIDINE DIHYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-(aminomethyl)-N-hydroxybenzimidamide → 4-(aminomethyl)benzenecarboximidamide (32797-61-8)

Guidance literature:

Pd-on-C; In methanol;

Reference yield: 99.0%

4-(aminomethyl)-N-hydroxybenzene-1-carboximidamide (328552-93-8) → 4-(aminomethyl)benzenecarboximidamide (32797-61-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 11h; under 2327.17 Torr;

DOI:10.1016/S0960-894X(02)00010-0

Reference yield:

4-(azidomethyl)benzonitrile (84466-87-5) → 4-(aminomethyl)benzenecarboximidamide (32797-61-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / H₂ / Pd/C / methanol; CHCl₃

2: HCl / 0 °C

3: NH₃ / methanol / 75 °C

With hydrogenchloride; ammonia; hydrogen; palladium on activated charcoal; In methanol; chloroform;

DOI:10.1016/j.bmcl.2004.07.054

upstream raw materials:

(4-carbamimidoyl-benzyl)-carbamic acid benzyl ester

4-(aminomethyl)-N-hydroxybenzene-1-carboximidamide

4-aminobenzyl cyanide

4-(azidomethyl)benzonitrile

Downstream raw materials:

C₂₀H₂₂N₄O₂S

C₂₇H₂₅N₁₁O₄S

C₁₆H₁₈N₆O₃S

C₂₁H₂₀N₆O₃S

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