3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

Base Information

Chemical Name:3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide
CAS No.:1393715-59-7
Molecular Formula:C₁₅H₁₀F₆OS
Molecular Weight:352.3
Hs Code.:

Synonyms:3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

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Chemical Property of 3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

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Technology Process of 3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

There total 5 articles about 3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 696-62-8
para-iodoanisole

: 130783-02-7
3,5-bis(trifluoromethyl)thiophenol

: 1393715-59-7
3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

Guidance literature:: With copper(l) iodide; trans-1,2-cyclohexandiol; potassium carbonate; In isopropyl alcohol; at 120 ℃; for 3h; Microwave irradiation;
DOI:10.3998/ark.5550190.0013.720

Reference yield: 81.0%

: 5335-87-5
4,4'-dimethoxyphenyl disulfide

: 402-31-3
1,3-bis(trifluoromethyl)benzene

: 1393715-59-7
3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

Guidance literature:: 1,3-bis(trifluoromethyl)benzene; With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; at 80 ℃; for 24h; Inert atmosphere;

4,4'-dimethoxyphenyl disulfide; With [2,2]bipyridinyl; copper(l) chloride; In water; dimethyl sulfoxide; at 80 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc33950a

Reference yield: 57.0%

: 696-63-9
4-Methoxybenzenethiol

: 328-73-4
3,5-bis(trifluoromethyl)iodobenzene

: 1393715-59-7
3,5-bis(tri?uoromethyl)phenyl 4-methoxyphenyl sulfide

Guidance literature:: 4-Methoxybenzenethiol; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Glovebox; Inert atmosphere; Sealed tube;

3,5-bis(trifluoromethyl)iodobenzene; With p-phenylpyridine; potassium methanolate; bis(pinacol)diborane; In dimethyl sulfoxide; at 25 ℃; for 24h; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1039/d1cc05294b