Technology Process of C47H77N7O14
There total 3 articles about C47H77N7O14 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C41H73NO11Si2; C17H32N5O6PolS; C42H77NO13Si2;
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
With
Oxone;
In
N,N-dimethyl-formamide;
at 20 ℃;
N-BOC-1,2-diaminoethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 1 h / 20 °C
2.1: ozone / dichloromethane / -68 °C
2.2: 14 h / 20 °C
3.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
3.2: 20 °C
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; ozone; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide;
2.2: Baeyer-Villiger Oxidation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ozone / dichloromethane / -68 °C
1.2: 14 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
2.2: 20 °C
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; ozone; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide;
1.2: Baeyer-Villiger Oxidation;