7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

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Chemical Name:7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole
CAS No.:1269631-54-0
Molecular Formula:C₅₀H₅₀N₂O₆
Molecular Weight:774.957
Hs Code.:

Synonyms:7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

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Chemical Property of 7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

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Technology Process of 7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

There total 25 articles about 7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1269631-53-9
4-(2-azido-3-tert-butoxyphenyl)-6-methoxy-2-(4-methoxybenzyl)-1-(4-methoxyphenethyl)-3,7-bis(4-methoxyphenyl)-1H-indole

: 1269631-54-0
7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

Guidance literature:: In 1,2-dichloro-benzene; for 0.666667h; Inert atmosphere; Reflux;
DOI:10.1002/asia.201000544

Reference yield:

: 1246523-61-4
(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

: 1269631-54-0
7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

Guidance literature:: With diisobutylaluminium hydride; In pentamethylbenzene,; toluene; at 20 ℃; for 2h;
DOI:10.1002/asia.201000544

Reference yield:

: 1246523-50-1
4-bromo-6-methoxy-3,7-bis-(4-methoxy-phenyl)-2,3-dihydro-1H-indole

: 1269631-54-0
7-tert-butoxy-5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazole

Guidance literature:: Multi-step reaction with 7 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 1 h / 20 °C

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 2 h

3.1: zinc(II) chloride / diethyl ether / 0 °C

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / Reflux

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / 1,4-dioxane; water / 1.5 h / 20 °C

6.1: 1,2-dichloro-benzene / 0.67 h / Reflux; Inert atmosphere

7.1: diisobutylaluminium hydride / pentamethylbenzene,; toluene / 2 h / 20 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; diisobutylaluminium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; sodium hydroxide; zinc(II) chloride; In 1,4-dioxane; diethyl ether; pentamethylbenzene,; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene; 5.1: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201000544