6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione

Base Information

• Chemical Name: 6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione
• CAS No.: 105199-53-9
• Molecular Formula: C₂₁H₁₇ClN₂O₂S
• Molecular Weight: 396.897

Synonyms:6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione

Chemical Property of 6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione

Chemical Property:

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Technology Process of 6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione

There total 4 articles about 6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Sodium; (4R,5S,6R)-4-(4-chloro-phenyl)-3-cyano-5-ethoxycarbonyl-6-hydroxy-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate (105199-43-7) → 6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(3H)-thione (105199-53-9)

Guidance literature:

With acetic acid; In water;

Reference yield:

C21H18ClN2O3S(1-)*C5H11N*H(1+) (111564-16-0) → 4-(p-Chlorophenyl)-6-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (105199-53-9,111564-18-2,111564-25-1) + 4-(p-Chlorophenyl)-6-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (105199-53-9,111564-18-2,111564-25-1)

Guidance literature:

With hydrogenchloride; In ethanol; Yield given; Heating;

DOI:10.1007/BF00475477

Reference yield:

C21H18ClN2O3S(1-)*C5H11N*H(1+) (111564-16-0) → 4-(p-Chlorophenyl)-6-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (105199-53-9,111564-18-2,111564-25-1) + 4-(p-Chlorophenyl)-6-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (105199-53-9,111564-18-2,111564-25-1)

Guidance literature:

With hydrogenchloride; In ethanol; Yield given; Heating;

DOI:10.1007/BF00475477

upstream raw materials:

C₂₁H₁₈ClN₂O₃S^(1-)*C₅H₁₁N*H⁽¹⁺⁾

Sodium; (4R,5S,6R)-4-(4-chloro-phenyl)-3-cyano-5-ethoxycarbonyl-6-hydroxy-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

(Z)-ethyl 2-benzoyl-3-(4'-chlorophenyl)-3-propenoate

Downstream raw materials:

2.2'-Bis(4-p-chlorophenyl-6-phenyl-5-ethoxycarbonyl-3-cyanopyridyl)-disulfide

4-(4-Chloro-phenyl)-5-cyano-2-phenyl-6-thioxo-1,6-dihydro-pyridine-3-carboxylic acid ethyl ester

2-methylthio-6-phenyl-4-(p-chlorophenyl)-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine

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