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[1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1H-indol-3-yl]-acetic acid tert-butyl ester

Base Information Edit
  • Chemical Name:[1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1H-indol-3-yl]-acetic acid tert-butyl ester
  • CAS No.:346424-36-0
  • Molecular Formula:C22H22ClNO4
  • Molecular Weight:399.874
  • Hs Code.:
  • Mol file:346424-36-0.mol
[1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1<i>H</i>-indol-3-yl]-acetic acid <i>tert</i>-butyl ester

Synonyms:[1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1H-indol-3-yl]-acetic acid tert-butyl ester

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Chemical Property of [1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1H-indol-3-yl]-acetic acid tert-butyl ester Edit
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SDS file from LookChem

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Technology Process of [1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1H-indol-3-yl]-acetic acid tert-butyl ester

There total 4 articles about [1-(4-chloro-benzoyl)-5-hydroxy-2-methyl-1H-indol-3-yl]-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen; acetic acid; palladium on activated charcoal; In ethyl acetate; for 3h; under 2888.19 Torr;
DOI:10.1021/jm000483h
Guidance literature:
Multi-step reaction with 3 steps
1.1: 62 percent / AcONa / acetic acid / 2 h / Heating
2.1: tBuOK / tetrahydrofuran / 0.33 h
2.2: 100 percent / tetrahydrofuran / 11 h
3.1: H2; AcOH / Pd/C / ethyl acetate / 3 h / 2888.19 Torr
With potassium tert-butylate; hydrogen; sodium acetate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; acetic acid; ethyl acetate;
DOI:10.1021/jm000483h
Guidance literature:
Multi-step reaction with 3 steps
1.1: 62 percent / AcONa / acetic acid / 2 h / Heating
2.1: tBuOK / tetrahydrofuran / 0.33 h
2.2: 100 percent / tetrahydrofuran / 11 h
3.1: H2; AcOH / Pd/C / ethyl acetate / 3 h / 2888.19 Torr
With potassium tert-butylate; hydrogen; sodium acetate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; acetic acid; ethyl acetate;
DOI:10.1021/jm000483h
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