{2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

Base Information

Chemical Name:{2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine
CAS No.:1251931-21-1
Molecular Formula:C₁₅H₁₉Br₂N₃O₂
Molecular Weight:433.143
Hs Code.:

Synonyms:{2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

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Technology Process of {2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

There total 3 articles about {2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1251931-20-0
4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenol

: 4584-46-7
(2-chloroethyl)dimethylamine hydrochloride

: 1251931-21-1
{2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.1016/j.bmc.2010.06.031

Reference yield:

: 1251931-20-0
4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenol

: 107-99-3
2-(dimethylamino)ethyl chloride

: 1251931-21-1
{2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.1016/j.bmc.2012.12.035

Reference yield:

: 22927-61-3
2,4,5-tribromo-1-methoxymethyl-1H-imidazole

: 1251931-21-1
{2-[4-(4,5-dibromo-1-methoxymethyl-1H-imidazol-2-yl)phenoxy]ethyl}dimethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / methanol; toluene / Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 40 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; caesium carbonate; In methanol; N,N-dimethyl-formamide; toluene; 1: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.12.035