N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

Base Information

Chemical Name:N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide
CAS No.:1050520-25-6
Molecular Formula:C₆₀H₆₆N₂O₆
Molecular Weight:911.194
Hs Code.:

Synonyms:N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

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Chemical Property of N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

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Technology Process of N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

There total 5 articles about N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 111-86-4
n-Octylamine

: 192126-74-2
[N,N'-dicyclohexyl-1,7-di(p-tert-butylphen-oxy)]perylene-3,4:9,10-tetracarboxylic dianhydride

: 1050520-25-6
N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

Guidance literature:: With 1H-imidazole; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1039/c4ce02392g

Reference yield:

: 98-54-4
para-tert-butylphenol

: 209111-67-1
N,N'-bis(n-octyl)-1,7-dibromo-perylene-3,4:9,10-bis(dicarboximide)

: 1050520-25-6
N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 130 ℃; for 12h; Inert atmosphere;
DOI:10.1002/bio.3537

Reference yield:

: 111-86-4
n-Octylamine

: 98-54-4
para-tert-butylphenol

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1246811-22-2
N,N'-dioctyl-1,6-di(2-tert-butylphenoxy)perylene-3,4,9,10-tetracarboxy diimide

: 1050520-25-6
N,N′‐dioctyl‐1,7‐di (4‐tert‐butylphenoxy)perylene‐3,4;9,10‐tetracarboxydiimide

Guidance literature:: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; With sulfuric acid; bromine; iodine; at 85 ℃; for 24h;

n-Octylamine; With propionic acid; for 48h; Reflux;

para-tert-butylphenol; With 18-crown-6 ether; potassium carbonate; In toluene; at 90 ℃; for 4h; Inert atmosphere;
DOI:10.1021/cm1018647