N-(3-Butyn-1-yl)-N-methylbenzamide

Base Information

Chemical Name:N-(3-Butyn-1-yl)-N-methylbenzamide
CAS No.:323581-00-6
Molecular Formula:C12H13 N O
Molecular Weight:187.241
Hs Code.:
DSSTox Substance ID:DTXSID20444669
Nikkaji Number:J1.447.959G
Wikidata:Q82262880
Mol file:323581-00-6.mol

Synonyms:323581-00-6;N-(3-Butyn-1-yl)-N-methylbenzamide;DTXSID20444669;N-Methyl-N-(3-butynyl)benzamide;N-(But-3-yn-1-yl)-N-methylbenzamide;Benzamide,N-3-butynyl-N-methyl-(9ci)

Suppliers and Price of N-(3-Butyn-1-yl)-N-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-(3-Butyn-1-yl)-N-methylbenzamide

Chemical Property:

PSA：20.31000
LogP:1.78190
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:187.099714038
Heavy Atom Count:14
Complexity:232

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(CCC#C)C(=O)C1=CC=CC=C1

Technology Process of N-(3-Butyn-1-yl)-N-methylbenzamide

There total 3 articles about N-(3-Butyn-1-yl)-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 323581-08-4
N-(but-3-yn-1-yl)benzamide

: 74-88-4
methyl iodide

: 323581-00-6
N-(but-3-ynyl)-N-methylbenzamide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 98-88-4
benzoyl chloride

: 323581-00-6
N-(but-3-ynyl)-N-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / Heating

2: LDA / tetrahydrofuran / 20 °C

With triethylamine; lithium diisopropyl amide; In tetrahydrofuran;

Reference yield:

: N-(but-3-ynyl)-N-chloromethylbenzamide

: 71785-91-6
(5,6-dihydropyridin-1(2H)-yl)(phenyl)methanone

: 323581-00-6
N-(but-3-ynyl)-N-methylbenzamide

: 323581-05-1
N-benzoyl-3-methylenepyrrolidine

Guidance literature:: With tri-n-butyl-tin hydride; 1,1'-azobis(1-cyanocyclohexanenitrile); In acetonitrile; for 1.5h; Product distribution; Heating;