benzylcarbamoyl cyanide

Base Information

• Chemical Name: benzylcarbamoyl cyanide
• CAS No.: 73708-69-7
• Molecular Formula: C₉H₈N₂O
• Molecular Weight: 160.175

Synonyms:benzylcarbamoyl cyanide

Chemical Property of benzylcarbamoyl cyanide

Chemical Property:

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Technology Process of benzylcarbamoyl cyanide

There total 8 articles about benzylcarbamoyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diethyl cyanophosphonate (2942-58-7) + carbon dioxide (124-38-9,18923-20-1) + benzylamine (100-46-9) → benzylcarbamoyl cyanide (73708-69-7)

Guidance literature:

With tetramethylphenylguanidine; In acetonitrile; at 0 ℃; for 1h;

DOI:10.1039/b912043b

Reference yield: 91.0%

carbon dioxide (124-38-9,18923-20-1) + Phosphorsaeure-diphenylestercyanid (51354-18-8) + benzylamine (100-46-9) → diphenyl benzyl(cyanocarbonyl)phosphoramidate (1195162-91-4) + 1,3-dibenzylimidazolidine-2,4,5-trione (21037-12-7) + benzylcarbamoyl cyanide (73708-69-7)

Guidance literature:

With tetramethylphenylguanidine; In acetonitrile; at 0 ℃; for 1h;

DOI:10.1039/b912043b

Reference yield: 89.0%

2-(hydroxyimino)-3-oxo-N-benzylbutanamide (77335-87-6) → benzylcarbamoyl cyanide (73708-69-7)

Guidance literature:

With trichlorophosphate; In 1,2-dichloro-ethane; at 80 ℃; for 2h;

DOI:10.1021/ol503643p

upstream raw materials:

carbonyl cyanide

benzylamine

diethyl cyanophosphonate

carbon dioxide

Downstream raw materials:

N-benzyl-N-(but-2-ynyl)cyanoformamide

N-benzyl-N-(pent-3-ynyl)cyanoformamide

N-benzyl-N-(5-phenylpent-4-ynyl)cyanoformamide

N-benzyl-N-(6-phenylhex-5-ynyl)cyanoformamide

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