Technology Process of N-Isopropyl-1,1,1-triphenylmethanesulfenamide
There total 4 articles about N-Isopropyl-1,1,1-triphenylmethanesulfenamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride; trifluoroacetic acid;
In
tetrahydrofuran;
Ambient temperature;
pH 4-5, indicator Bromocresol Green;
DOI:10.1021/jo00168a031
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 88 percent / Sulfuryl chloride / toluene; diethyl ether / 2 h / 0 °C
2: 78 percent / 29 percent NH4OH/H2O / CH2Cl2 / 0 °C
3: 98 percent / Pridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO4 / CH2Cl2 / 2 h / Ambient temperature
4: 98 percent / NaBH3CN/1percent CF3COOH / tetrahydrofuran / Ambient temperature; pH 4-5, indicator Bromocresol Green
With
ammonium hydroxide; sulfuryl dichloride; water; pyridinium p-toluenesulfonate; sodium cyanoborohydride; magnesium sulfate; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00168a031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78 percent / 29 percent NH4OH/H2O / CH2Cl2 / 0 °C
2: 98 percent / Pridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO4 / CH2Cl2 / 2 h / Ambient temperature
3: 98 percent / NaBH3CN/1percent CF3COOH / tetrahydrofuran / Ambient temperature; pH 4-5, indicator Bromocresol Green
With
ammonium hydroxide; water; pyridinium p-toluenesulfonate; sodium cyanoborohydride; magnesium sulfate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00168a031
