P(C₆H₅)4⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = P(C₆H₅)4[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O

Base Information

• Chemical Name: P(C₆H₅)4⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = P(C₆H₅)4[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O
• CAS No.: 85082-27-5
• Molecular Formula: C₁₂H₈N₂O₇V*C₂₄H₂₀P*H₂O
• Molecular Weight: 700.558

Synonyms:P(C₆H₅)4⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = P(C₆H₅)4[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O

Chemical Property of P(C₆H₅)4⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = P(C₆H₅)4[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O

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Technology Process of P(C₆H₅)4⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = P(C₆H₅)4[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O

There total 3 articles about P(C₆H₅)4⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = P(C₆H₅)4[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Picolinic acid (98-98-6) + ammonium vanadate(V) + tetraphenylphosphonium bromide (2751-90-8) → P(C6H5)4(1+)*VO(O2)(C5H4(CO2)N)2(1-)*H2O = P(C6H5)4[VO(O2)(C5H4(CO2)N)2]*H2O (85082-27-5)

Guidance literature:

With H₂O₂; In dichloromethane; dissolving NH4VO3 and picolinic acid in 30 % H2O2 at 0°C for 1 h; addn. of tetraphenylphosphonium bromide; filtration; washing (H2O, diethyl ether); elem. anal.;

DOI:10.1021/ja00348a025

Reference yield:

H(1+)*VO(O2)(C5H4(CO2)N)2(1-)*H2O = H[VO(O2)(C5H4(CO2)N)2]*H2O (85082-24-2) + tetraphenylphosphonium bromide (2751-90-8) → P(C6H5)4(1+)*VO(O2)(C5H4(CO2)N)2(1-)*H2O = P(C6H5)4[VO(O2)(C5H4(CO2)N)2]*H2O (85082-27-5)

Guidance literature:

In water;

DOI:10.1021/ja00348a025

Reference yield:

<(pyridine-2-carboxylate)2VO(O2)>-H+*HMPT (85082-25-3) + tetraphenylphosphonium bromide (2751-90-8) → P(C6H5)4(1+)*VO(O2)(C5H4(CO2)N)2(1-)*H2O = P(C6H5)4[VO(O2)(C5H4(CO2)N)2]*H2O (85082-27-5)

Guidance literature:

In water;

DOI:10.1021/ja00348a025

upstream raw materials:

<(pyridine-2-carboxylate)2VO(O2)>^-H⁺*HMPT

tetraphenylphosphonium bromide

H⁽¹⁺⁾*VO(O₂)(C₅H₄(CO₂)N)2^(1-)*H₂O = H[VO(O₂)(C₅H₄(CO₂)N)2]*H₂O

2-Picolinic acid

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