(1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

Base Information

Chemical Name:(1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide
CAS No.:145450-35-7
Molecular Formula:C₂₄H₃₆NO₂*I
Molecular Weight:497.46
Hs Code.:

Synonyms:(1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

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Chemical Property of (1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

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Technology Process of (1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

There total 4 articles about (1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 145450-34-6
(1R,2S)-2-Phenyl-cyclohexanecarboxylic acid (1R,3R,5S)-8-isopropyl-8-aza-bicyclo[3.2.1]oct-3-yl ester

: 74-88-4
methyl iodide

: 145450-35-7
(1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

Guidance literature:: In acetonitrile; at 50 ℃; for 3h;
DOI:10.1016/0223-5234(92)90179-5

Reference yield:

: 3423-25-4
endo-8-(1-methylethyl)-8-azabicyclo<3.2.1>octan-3-ol

: 145450-35-7
(1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / triethylamine / 1,2-dichloro-ethane / 9 h / Heating

2: 84 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr / Ambient temperature

3: 60 percent / acetonitrile / 3 h / 50 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/0223-5234(92)90179-5

Reference yield:

: 145450-39-1
2-phenyl-2-cyclohexene-1-carbonyl chloride

: 145450-35-7
(1R,3R,5S,8R)-8-Isopropyl-8-methyl-3-((1R,2S)-2-phenyl-cyclohexanecarbonyloxy)-8-azonia-bicyclo[3.2.1]octane; iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / triethylamine / 1,2-dichloro-ethane / 9 h / Heating

2: 84 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr / Ambient temperature

3: 60 percent / acetonitrile / 3 h / 50 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/0223-5234(92)90179-5